Synthesis of Betsylated Amino Acids Using Aqueous Buffered Sodium Hypochlorite Solution

A Safer, Scalable Route to Betsylated Amino Acids for Peptide Synthesis

Explore a new, efficient method to synthesize N-Bts-protected amino acids from unprotected precursors in a single step—without hazardous reagents. Using sodium betsylate and buffered NaOCl, this scalable process enables the clean isolation of high-yield peptide building blocks suitable for both solution and solid-phase peptide synthesis (SPPS).

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